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Moon-Sung Cho 1 Article
Effect of Deposition Temperature on the Property of Pyrolytic SiC Fabricated by the FBCVD Method
Yeon-Ku Kim, Weon-Ju Kim, SungHwan Yeo, Moon-Sung Cho
J Powder Mater. 2014;21(6):434-440.   Published online December 1, 2014
DOI: https://doi.org/10.4150/KPMI.2014.21.6.434
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AbstractAbstract PDF

Silicon carbide(SiC) layer is particularly important tri-isotropic (TRISO) coating layers because it acts as a miniature pressure vessel and a diffusion barrier to gaseous and metallic fission products in the TRISO coated particle. The high temperature deposition of SiC layer normally performed at 1500-1650°C has a negative effect on the property of IPyC layer by increasing its anisotropy. To investigate the feasibility of lower temperature SiC deposition, the influence of deposition temperature on the property of SiC layer are examined in this study. While the SiC layer coated at 1500°C obtains nearly stoichiometric composition, the composition of the SiC layer coated at 1300-1400°C shows discrepancy from stoichiometric ratio(1:1). 3-7 μm grain size of SiC layer coated at 1500°C is decreased to sub-micrometer (<1 μm) -2 μm grain size when coated at 1400°C, and further decreased to nano grain size when coated at 1300- 1350°C. Moreover, the high density of SiC layer (≥3.19 g/cm3) which is easily obtained at 1500°C coating is difficult to achieve at lower temperature owing to nano size pores. the density is remarkably decreased with decreasing SiC deposition temperature.

Citations

Citations to this article as recorded by  
  • High-temperature thermo-mechanical behavior of functionally graded materials produced by plasma sprayed coating: Experimental and modeling results
    Kang Hyun Choi, Hyun-Su Kim, Chang Hyun Park, Gon-Ho Kim, Kyoung Ho Baik, Sung Ho Lee, Taehyung Kim, Hyoung Seop Kim
    Metals and Materials International.2016; 22(5): 817.     CrossRef

Journal of Powder Materials : Journal of Powder Materials